Caustic soda Hot water White clay vacuum Recycled water
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Crude oil → Alkali refining → Degumming → Bleaching → Deodorize → Cool down → Deodorized oil → Go to the dewaxing workshop
(2) Process flow description
①Alkali refining operation: adjust the oil temperature to about 60℃, then add 20-30Be lye (1kg caustic soda + 5kg water lye) within 5-10min, and stir for 5-10min under the condition of 60r/min, Observe the formation and separation of soap particles after the reaction and start to slowly heat up, change to slow stirring, and increase by about 1°C every minute. When the temperature reaches 65°C, the oil soap separates obviously, stop stirring and start to settle the soap feet. Generally, it is necessary Soap feet are released after 4-6 hours.
②Washing operation: After the soapstock is released, the oil is further heated to 75°C, and then hot water greater than 5% of the oil weight is added for washing. The water temperature should be 5-10°C higher than the oil temperature, and the water temperature should be 5-10°C higher than the oil temperature. It is easy to emulsify when the water temperature is too low; After adding water, continue to stir for 5 minutes, and then settle for 3-4 hours, release soapy water, and wash repeatedly 1-2 times, depending on the quality of the clear oil.
③Decolorization operation: turn on the vacuum pump to make the vacuum ≧700mmHg; first suck the washed alkali refining oil into the decolorization tank, turn on the stirring and increase the temperature under the vacuum state, and continue to stir for 10 minutes after the temperature reaches 100℃ to reduce the water content in the oil to 0.1% Below, inhale a small amount of decolorizing agent (white clay or activated carbon), the amount of addition depends on the oil product, generally 2%-4% of the oil amount, after stirring for 20 minutes, the temperature is cooled to about 90°C, the vacuum is broken, and the decolorization pump is turned on to filter The machine separates oil and soil to obtain decolorized oil.
④Deodorization operation: the decolorized oil is sucked into the deodorization tank by a vacuum. When the vacuum degree reaches 755mmHg and the temperature is above 150℃, the bottom is opened and the steam is directly distilled and deodorized, and the timing is started;
A. deodorization time: 2-3h,
B. Deodorization temperature: 220℃-240℃,
C. deodorization vacuum degree: 755mmHg or more,
D. The whole process must be directly steam distilled.
6. Description of main equipment:
Serial number |
Device name |
Quantity |
Description |
1 |
Refining tank |
2 |
Used for acid refining, alkali refining and water washing |
2 |
Decolorizing tank |
1 |
Used for dehydration, mixing oil and decolorant |
3 |
Deodorization tank |
1 |
It is made of 304 stainless steel and used for distillation to remove oil odor and light components |
4 |
Vacuum pump |
1 |
The vacuum needed for decolorization and deodorization can reach 755irfg |
5 |
Air compressor |
1 |
Drying bleaching clay |
6 |
Steam generator |
1 |
Generate steam for distillation |
7 |
Filter |
1 |
Filtration separation of clay oil |
8 |
Heat conducting oil furnace |
1 |
Provide system heat energy,temperature can reach 300℃ |
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